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Elektroanalysis - fundamentals and applications.

General data

Course ID: 1600-DUER2EL
Erasmus code / ISCED: (unknown) / (0531) Chemistry The ISCED (International Standard Classification of Education) code has been designed by UNESCO.
Course title: Elektroanalysis - fundamentals and applications.
Name in Polish: Electroanalysis - fundamentals and applications.
Organizational unit: Faculty of Chemistry
Course groups:
ECTS credit allocation (and other scores): 0 OR 4.00 (depends on study program) Basic information on ECTS credits allocation principles:
  • the annual hourly workload of the student’s work required to achieve the expected learning outcomes for a given stage is 1500-1800h, corresponding to 60 ECTS;
  • the student’s weekly hourly workload is 45 h;
  • 1 ECTS point corresponds to 25-30 hours of student work needed to achieve the assumed learning outcomes;
  • weekly student workload necessary to achieve the assumed learning outcomes allows to obtain 1.5 ECTS;
  • work required to pass the course, which has been assigned 3 ECTS, constitutes 10% of the semester student load.
view allocation of credits
Language: English
Prerequisits:

Fundamentals of electrochemistry, basic electroanalytical methods, redox processes of organic and inorganic compounds.
Short description:

The aim of the lecture is to provide Students in English with in-depth knowledge of electroanalytical chemistry, advanced electroanalytical techniques as well as various aspects of charge transfer processes, electrode reaction mechanisms and the application of electrocatalytic processes in electroanalysis.

The subjects of lecture are:

1. Electrode reactions.

2. Kinetics of heterogenic electron transfer and mass transport.

3. Electrical double layer and its structure.

4. Thermodynamics and kinetics of electrochemical reactions.

5. Electrodes, electrolytes and experimental setup.

Discussed Electroanalytical Techniques

6. Potentiometry.

7. Cyclic voltammetry .

8. Pulse voltammetry

9. Square-wave voltammetry .

10. Chronocoulometry.

11. Electrochemical impedance spectroscopy.

12. UV/Vis/NIR spectroelectrochemistry.

13. Stripping voltammetry.

14. Electrochemical studies of solid compounds and materials.

15. Electrochemical quartz crystal microbalance.
Learning outcomes:

Knowledge

1. Has knowledge of basic electroanalytical concepts and theories (16C-1A_W05, 16K-1_W05, 16A-1A_W05)

2. Knows the computational methods used to solve basic problems in the field of electroanalysis and examples of their practical use (16C-1A_W01, 16C-1A_W04, 16K-1_W01, 16K-1_W04, 16A-1A_W01, 16A-1A_W04)

3. Knows the basics of construction and operation of the apparatus used in electroanalysis (16C-1A_W10, 16K-1_W10, 16A-1A_W06)

Skills

1. Can present in speech and writing the basic issues concerning: the construction of the electrochemical layer, the theory of electrode and electrocatalytic processes, basic electroanalytical methods, (16C-1A_U01, 16K-1_U01, 16A-1A_U14)

2. Can present the basic electrode processes and their mechanisms in inorganic and organic chemistry (16C-1A_U10, 16K-1_U10, 16A-1A_U16)

3. Can read basic parameters from the results of electroanalytical measurements and can perform basic electroanalytical calculations (16C-1A_U07, 16K-1_U07, 16A-1A_U02)

4. Can interpret the results of electroanalytical measurements (16C-1A_U07, 16K-1_U07, 16A-1A_U02)

5. Is able to use the software to analyze the results of electroanalytical measurements. (16C-1A_U08, 16K-1_U08, 16A-1A_U04)

6. Can plan electroanalytical measurement (16C-1A_U01, 16C-1A_U02, 16K-1_U01, 16K-1_U02, 16A-1A_U05)

7. Can relate her/his knowledge in the field of electroanalysis to other areas of chemistry and related sciences. (16C-1A_U04, 16K-1_U04, 16A-1A_U16)

8. Can describe the construction and operation of electroanalytical equipment. (16C-1A_U01, 16K-1_U01, 16A-1A_U14)

9. Can search for information on a given topic using various sources of scientific information in English and present it in the form of a prepared document. (16K-1_U09, 16K-1_U03, 16K-1_U09, 16K-1_U03, 16A-1A_U06, 16A-1A_U13)

Social competences

1. Can cooperate and work in a group and is aware of the responsibility for the tasks performed by the team, (16C-1A_K03, 16C-1A_K05, 16K-1_K03, 16K-1_K05, 16A-1A_K02, 16A-1A_K03)

2. Understands the need to improve professional and personal competences, understands the need to combine knowledge from various fields to solve the problem (16C-1A_K05, 16K-1_K05, 16A-1A_K03, 16A-1A_K04)

3. Can formulate opinions and argue in their favor. (16C-1A_K07, 16K-1_K07, 16A-1A_K05

Classes in period "Summer Semester 2024/2025" (future)

Time span: 2025-02-17 - 2025-09-30
Selected timetable range:
Navigate to timetable
Type of class:
Examination more information
Lecture, 28 hours more information
Coordinators: Sławomir Domagała
Group instructors: (unknown)
Students list: (inaccessible to you)
Examination: (in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:

(in Polish) T

Classes in period "Summer Semester 2023/2024" (in progress)

Time span: 2024-02-26 - 2024-09-30
Selected timetable range:
Navigate to timetable
Type of class:
Examination more information
Lecture, 28 hours more information
Coordinators: Sławomir Domagała
Group instructors: Sławomir Domagała
Students list: (inaccessible to you)
Examination: (in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:

(in Polish) T

Classes in period "Summer Semester 2022/2023" (past)

Time span: 2023-02-20 - 2023-09-30
Selected timetable range:
Navigate to timetable
Type of class:
Examination more information
Lecture, 28 hours more information
Coordinators: Sławomir Domagała
Group instructors: (unknown)
Students list: (inaccessible to you)
Examination: (in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:

(in Polish) T

Classes in period "Summer Semester 2021/2022" (past)

Time span: 2022-02-21 - 2022-09-30
Selected timetable range:
Navigate to timetable
Type of class:
Examination more information
Lecture, 28 hours more information
Coordinators: Sławomir Domagała
Group instructors: Sławomir Domagała
Students list: (inaccessible to you)
Examination: (in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:

(in Polish) T
Teaching Method:

Lecture - Power Point presentation (information lecture and problem lecture)
Method and Criteria of Assessment:

Written exam in English (obtaining 50% of the possible points)
(in Polish) Metody weryfikacji i oceny stopnia osiągnięcia założonych efektów uczenia się:

Active participation in classes

Case study

Discussion

Knowledge map

Exam
Course Content:

The aim of the lecture is to provide Students in English with in-depth knowledge of electroanalytical chemistry, advanced electroanalytical techniques as well as various aspects of charge transfer processes, electrode reaction mechanisms and the application of electrocatalytic processes in electroanalysis.


The subjects of lecture are:

1. Electrode reactions.

2. Kinetics of heterogenic electron transfer and mass transport.

3. Electrical double layer and its structure.

4. Thermodynamics and kinetics of electrochemical reactions.

5. Electrodes, electrolytes and experimental setup.

Discussed Electroanalytical Techniques

6. Potentiometry.

7. Cyclic voltammetry .

8. Pulse voltammetry

9. Square-wave voltammetry .

10. Chronocoulometry.

11. Electrochemical impedance spectroscopy.

12. UV/Vis/NIR spectroelectrochemistry.

13. Stripping voltammetry.

14. Electrochemical studies of solid compounds and materials.

15. Electrochemical quartz crystal microbalance.
Bibliography:

1. C. Lefrou, P. Fabry, J.C. Poignet, “Electrochemistry”, Springer, 2012

2. J. Bard, L.R. Faulkner, “Electrochemical Methods - Fundamentals and Applications”, Wiley, 2001

3. H. Lund, “Organic Electrochemistry”, Marcel Dekker, 2001

4. J. Wang, Analytical Electrochemistry , Marcel Dekker, New York, Basel, 2001

Classes in period "Summer Semester 2020/2021" (past)

Time span: 2021-03-08 - 2021-09-30
Selected timetable range:
Navigate to timetable
Type of class:
Examination more information
Lecture, 28 hours more information
Coordinators: Sławomir Domagała
Group instructors: Sławomir Domagała
Students list: (inaccessible to you)
Examination: Course - (in Polish) Ocena zgodna z regulaminem studiów
Examination - (in Polish) Ocena zgodna z regulaminem studiów
Lecture - (in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:

(in Polish) T
Teaching Method:

Feeding methods - informative and problem lecture with the elements of multimedia presentations.
Method and Criteria of Assessment:

The grade of the written exam (100%) evaluating the effects of training in the skills (e1-e10).
Course Content:

The subjects of lecture are:


1. Oxidation and reduction processes.

2. Electrode reactions.

3. Kinetics of heterogenic electron transfer and mass transport.

4. Electrical double layer and its structure.

5. Thermodynamics of electrochemical reactions

6. Kinetics of electrochemical reactions.

7. Electrodes, electrolytes and experimental setup.

8. Potentiometry.

9. Cyclic voltammetry .

10. Pulse voltammetry

11. Square-wave voltammetry .

12. Chronocoulometry.

13. Electrochemical impedance spectroscopy.

14. UV/Vis/NIR spectroelectrochemistry.

15. Stripping voltammetry.

16. Electrochemical studies of solid compounds and materials.

17. Electrochemical quartz crystal nanobalance.
Bibliography:

A. Bard, Electrochemical Methods: Fundamentals and Applications, John Wiley & Sons, 2001

H. Lund, Organic Electrochemistry, Marcel Dekker, New York, Basel, 2001

I. Fried, The chemistry of electrode processes. Academic Press London and New York, 1973

J. Wang, Analytical Electrochemistry , Marcel Dekker, New York, Basel, 2001

Classes in period "Summer Semester 2019/2020" (past)

Time span: 2020-02-24 - 2020-09-30
Selected timetable range:
Navigate to timetable
Type of class:
Examination more information
Lecture, 28 hours more information
Coordinators: Sławomir Domagała
Group instructors: Sławomir Domagała
Students list: (inaccessible to you)
Examination: Course - (in Polish) Ocena zgodna z regulaminem studiów
Examination - (in Polish) Ocena zgodna z regulaminem studiów
Lecture - (in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:

(in Polish) T
Teaching Method:

Feeding methods - informative and problem lecture with the elements of multimedia presentations.
Method and Criteria of Assessment:

The grade of the written exam (100%) evaluating the effects of training in the skills (e1-e10).
Course Content:

The subjects of lecture are:


1. Oxidation and reduction processes.

2. Electrode reactions.

3. Kinetics of heterogenic electron transfer and mass transport.

4. Electrical double layer and its structure.

5. Thermodynamics of electrochemical reactions

6. Kinetics of electrochemical reactions.

7. Electrodes, electrolytes and experimental setup.

8. Potentiometry.

9. Cyclic voltammetry .

10. Pulse voltammetry

11. Square-wave voltammetry .

12. Chronocoulometry.

13. Electrochemical impedance spectroscopy.

14. UV/Vis/NIR spectroelectrochemistry.

15. Stripping voltammetry.

16. Electrochemical studies of solid compounds and materials.

17. Electrochemical quartz crystal nanobalance.
Bibliography:

A. Bard, Electrochemical Methods: Fundamentals and Applications, John Wiley & Sons, 2001

H. Lund, Organic Electrochemistry, Marcel Dekker, New York, Basel, 2001

I. Fried, The chemistry of electrode processes. Academic Press London and New York, 1973

J. Wang, Analytical Electrochemistry , Marcel Dekker, New York, Basel, 2001

Classes in period "Summer Semester 2018/2019" (past)

Time span: 2019-02-18 - 2019-09-30
Selected timetable range:
Navigate to timetable
Type of class:
Examination more information
Lecture, 28 hours more information
Coordinators: Sławomir Domagała
Group instructors: Sławomir Domagała
Students list: (inaccessible to you)
Examination: Course - (in Polish) Ocena zgodna z regulaminem studiów
Examination - (in Polish) Ocena zgodna z regulaminem studiów
Lecture - (in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:

(in Polish) T
Teaching Method:

Feeding methods - informative and problem lecture with the elements of multimedia presentations.
Method and Criteria of Assessment:

The grade of the written exam (100%) evaluating the effects of training in the skills (e1-e10).
Course Content:

The subjects of lecture are:


1. Oxidation and reduction processes.

2. Electrode reactions.

3. Kinetics of heterogenic electron transfer and mass transport.

4. Electrical double layer and its structure.

5. Thermodynamics of electrochemical reactions

6. Kinetics of electrochemical reactions.

7. Electrodes, electrolytes and experimental setup.

8. Potentiometry.

9. Cyclic voltammetry .

10. Pulse voltammetry

11. Square-wave voltammetry .

12. Chronocoulometry.

13. Electrochemical impedance spectroscopy.

14. UV/Vis/NIR spectroelectrochemistry.

15. Stripping voltammetry.

16. Electrochemical studies of solid compounds and materials.

17. Electrochemical quartz crystal nanobalance.
Bibliography:

A. Bard, Electrochemical Methods: Fundamentals and Applications, John Wiley & Sons, 2001

H. Lund, Organic Electrochemistry, Marcel Dekker, New York, Basel, 2001

I. Fried, The chemistry of electrode processes. Academic Press London and New York, 1973

J. Wang, Analytical Electrochemistry , Marcel Dekker, New York, Basel, 2001

Classes in period "Summer Semester 2017/2018" (past)

Time span: 2018-02-19 - 2018-09-30
Selected timetable range:
Navigate to timetable
Type of class:
Examination more information
Lecture, 28 hours more information
Coordinators: Sławomir Domagała
Group instructors: Sławomir Domagała
Students list: (inaccessible to you)
Examination: Course - (in Polish) Ocena zgodna z regulaminem studiów
Examination - (in Polish) Ocena zgodna z regulaminem studiów
Lecture - (in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:

(in Polish) T
Teaching Method:

Feeding methods - informative and problem lecture with the elements of multimedia presentations.
Method and Criteria of Assessment:

The grade of the written exam (100%) evaluating the effects of training in the skills (e1-e10).
Course Content:

The subjects of lecture are:


1. Oxidation and reduction processes.

2. Electrode reactions.

3. Kinetics of heterogenic electron transfer and mass transport.

4. Electrical double layer and its structure.

5. Thermodynamics of electrochemical reactions

6. Kinetics of electrochemical reactions.

7. Electrodes, electrolytes and experimental setup.

8. Potentiometry.

9. Cyclic voltammetry .

10. Pulse voltammetry

11. Square-wave voltammetry .

12. Chronocoulometry.

13. Electrochemical impedance spectroscopy.

14. UV/Vis/NIR spectroelectrochemistry.

15. Stripping voltammetry.

16. Electrochemical studies of solid compounds and materials.

17. Electrochemical quartz crystal nanobalance.
Bibliography:

A. Bard, Electrochemical Methods: Fundamentals and Applications, John Wiley & Sons, 2001

H. Lund, Organic Electrochemistry, Marcel Dekker, New York, Basel, 2001

I. Fried, The chemistry of electrode processes. Academic Press London and New York, 1973

J. Wang, Analytical Electrochemistry , Marcel Dekker, New York, Basel, 2001
Course descriptions are protected by copyright.
Copyright by UNIVERSITY OF LODZ.
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