UNIVERSITY OF LODZ - Central Authentication System

Instrumental Analysis

General data

Course ID:	1600-DUER1In
Erasmus code / ISCED:	(unknown) / (0531) Chemistry The ISCED (International Standard Classification of Education) code has been designed by UNESCO.
Course title:	Instrumental Analysis
Name in Polish:	Instrumental Analysis
Organizational unit:	Faculty of Chemistry
Course groups:
ECTS credit allocation (and other scores):	0 OR 8.00 (depends on study program) Basic information on ECTS credits allocation principles: the annual hourly workload of the student’s work required to achieve the expected learning outcomes for a given stage is 1500-1800h, corresponding to 60 ECTS; the student’s weekly hourly workload is 45 h; 1 ECTS point corresponds to 25-30 hours of student work needed to achieve the assumed learning outcomes; weekly student workload necessary to achieve the assumed learning outcomes allows to obtain 1.5 ECTS; work required to pass the course, which has been assigned 3 ECTS, constitutes 10% of the semester student load. view allocation of credits
Language:	English
Prerequisits:	1. Student is familiar with the theoretical basis of spetrophotometry, potentiometry and conductometry Student can develop a strategy to solve complex measurement problems using above memtion analytical instrumental techniques. Student can assess the capabilities and limitations of these techniques of instrumental analysis.
Short description:	Objectives of course: Obtaining skills in the range of basic techniques of instrumental analysis.
Learning outcomes:	Knowledge: I_W01:Student is familiar with the theoretical basis of spectroscopic, electrochemical, enzymatic and separation techniques. (16K2C_W03; 16K2C_W04) I_W02:Student knows the basic aspects of the design and operation of equipment used in spectroscopic, electrochemical, enzymatic and separation techniques. (16K2C_W04) I_W03:Student has expertise in sample preparation to final analysis. (16K2C_W05) Skills: I_U01:Student knows how to formulate the basis of measurement techniques in modern analytical laboratories. (16K2C_W03; 16K2C_U01) I_U02:Student can assess the capabilities and limitations of these techniques of instrumental analysis. (16K2C_W03ł 16K2C_U01) I_U03:Student is able to develop complex measurement strategy to solve complex problems using known analytical instrumental techniques. (16K2C_U01) I_U04:Student can apply appropriate statistical methods allow statistical evaluation of the results. (16K2C_W02; 16K2C_U01; 16K2C_U03) I_U05:Student analyze critically the results and present them in a report. (16K2C_W02; 16K2C_U03) Social competence: I_K01:Able to work in a team. (16K2C_K04) I_K02:He can formulate opinions on the chemical analysis. (16K2C_K07) I_K03:Have a sense of responsibility for collaborative tasks related to teamwork. (16K2C_K04)

Classes in period "Winter Semester 2024/2025" (future)

Time span:	2024-10-01 - 2025-02-16	Selected timetable range: weekly course term Navigate to timetable
Type of class:	Discussion class, 28 hours more information Examination more information Laboratory, 56 hours more information Lecture, 14 hours more information
Coordinators:	Sławomir Domagała
Group instructors:	(unknown)
Students list:	(inaccessible to you)
Examination:	(in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:	(in Polish) T

Classes in period "Winter Semester 2023/2024" (past)

Time span:	2023-10-01 - 2024-02-25	Selected timetable range: weekly course term Navigate to timetable
Type of class:	Discussion class, 28 hours more information Examination more information Laboratory, 56 hours more information Lecture, 14 hours more information
Coordinators:	Sławomir Domagała
Group instructors:	(unknown)
Students list:	(inaccessible to you)
Examination:	(in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:	(in Polish) T

Classes in period "Winter Semester 2022/2023" (past)

Time span:	2022-10-01 - 2023-02-19	Selected timetable range: weekly course term Navigate to timetable
Type of class:	Discussion class, 28 hours more information Examination more information Laboratory, 56 hours more information Lecture, 14 hours more information
Coordinators:	Sławomir Domagała
Group instructors:	(unknown)
Students list:	(inaccessible to you)
Examination:	(in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:	(in Polish) T

Classes in period "Winter Semester 2021/2022" (past)

Time span:	2021-10-01 - 2022-01-23	Selected timetable range: weekly course term Navigate to timetable
Type of class:	Discussion class, 28 hours more information Examination more information Laboratory, 56 hours more information Lecture, 14 hours more information
Coordinators:	Sławomir Domagała
Group instructors:	(unknown)
Students list:	(inaccessible to you)
Examination:	(in Polish) Ocena zgodna z regulaminem studiów
(in Polish) Czy IRK BWZ?:	(in Polish) T

Classes in period "Winter Semester 2020/2021" (past)

Time span:	2020-10-01 - 2021-02-07	Selected timetable range: weekly course term Navigate to timetable
Type of class:	Discussion class, 28 hours more information Examination more information Laboratory, 56 hours more information Lecture, 14 hours more information
Coordinators:	Sławomir Domagała
Group instructors:	Sławomir Domagała
Students list:	(inaccessible to you)
Examination:	Course - (in Polish) Ocena zgodna z regulaminem studiów Discussion class - (in Polish) Ocena zgodna z regulaminem studiów Examination - (in Polish) Ocena zgodna z regulaminem studiów Laboratory - (in Polish) Ocena zgodna z regulaminem studiów Lecture - (in Polish) Zaliczenie lub ocena
(in Polish) Czy IRK BWZ?:	(in Polish) T
Teaching Method:	Lecture: a method of verbal-enriched multimedia presentation. Laboratory: practical method, the execution of the planned exercises, conversation. Seminar: word method, talk, presentation of papers prepared using multimedia support and discussion.
Method and Criteria of Assessment:	Assessment: Lecture: written exam at the end of semester Proseminar: passing 2 writing colloquiums, attendance in class Laboratory: passing 2 writing colloquiums and the workmanship of 9 laboratory tasks The final grade is a weighted average of the ratings of the test (50%), laboratory (25%), seminar (25%).
Course Content:	1.Calibration techniques: analytical calibration curve, method of standard additions. 2. Accuracy and precision, selectivity and sensitivity. 3. Separation techniques: general principles (retention, column efficiency, number of theoretical plates, van Deemetrs equation), classification of chromatographic methods. Gas chromatography (GC): columns and stationary phases, detectors, sample introduction system, qualitative and quantitative analysis. Temperature program, pyrolysis gas chromatography, applications. High performance liquid chromatography (HPLC): columns and stationary phases, solvents and choice of solvent systems in ion, partition, gel and adsorption chromatography, pumps, sample introduction systems, detectors, isocratic and gradient elution, qualitative and quantitative analysis. Ion chromatography: ion exchange, mobile phases, supresors, detectors. Supercritical fluid chromatography: principles and instrumentation. Electrophoresis: principles and instrumentation (capillary, buffer, detection) for CE 4. Spectrometry (spectrophotometry, AAS, AES): interaction of electromagnetic radiation with matter, electronic spectra and molecular structure, the basic notions and absorption laws, the choice of the wavelength, spectrometric methods of quantitative analysis. Analytical application of spectrophotometry. Speciation analysis. Atomic spectroscopy: principles (sources of atomic spectra) and instrumentation for spectrometric methods Atomic absorption spectroscopy: sample atomization and atomizers (flame atomization, electrothetmal atomization), atomization stages, radiation sources (hollow cathode lamps, electrodeless discharge lamps), interferences. Atomic emission spectroscopy: flame emission spectrometry, emission spectroscopy based upon plasma (inductively coupled plasma ICP), arc and spark atomization. 5. Analytical application of conductometry. Direct conductometry and conductometric titration. Analytical application of potentiometric measurements. Direct potentiometry, pehametry, potentiometric titration. 6. Electrogravimetry and coulometry: Faraday’s laws, potentiostatic and amperostatic coulometry, application of coulometric titration. 7. Polarograpic and voltammetric methods: classification of polarographic and voltammetric techniques, electrodes (HMDE, DME, SMDE, solid electrodes), polarograms, voltammograms, voltammetric currents, the basic notions (DME, polarizable electrode, over-voltage, half-wave (peak) potential, depolarizier, Ilkovic equation), currents in polarography, the supporting electrolyte, alternating current polarography, normal-pulse polarography, differential pulse polarography, square-wave polarography, principles and application of normal pulse, differential pulse, quare-wave and cyclic voltammetry, principles and application of stripping methods (anodic and cathodic stripping techniques, adsorptive stripping techniques).
Bibliography:	D. A. Skoog „Principles of Instrumental Analysis” H. H. Willard, L. L. Merritt, J. A. Dean, F. A. Settle “Instrumental Methods of Analysis” Gary D. Christian „Analytical Chemistry”, John Wiley & Sons, INC.

Classes in period "Winter Semester 2019/2020" (past)

Time span:	2019-10-01 - 2020-02-23	Selected timetable range: weekly course term Navigate to timetable
Type of class:	Discussion class, 28 hours more information Examination more information Laboratory, 56 hours more information Lecture, 14 hours more information
Coordinators:	Sławomir Domagała
Group instructors:	Kamila Borowczyk, Sławomir Domagała, Justyna Piechocka, Łukasz Półtorak
Students list:	(inaccessible to you)
Examination:	Course - (in Polish) Ocena zgodna z regulaminem studiów Discussion class - (in Polish) Ocena zgodna z regulaminem studiów Examination - (in Polish) Ocena zgodna z regulaminem studiów Laboratory - (in Polish) Ocena zgodna z regulaminem studiów Lecture - (in Polish) Zaliczenie lub ocena
(in Polish) Czy IRK BWZ?:	(in Polish) T
Teaching Method:	Lecture: a method of verbal-enriched multimedia presentation. Laboratory: practical method, the execution of the planned exercises, conversation. Seminar: word method, talk, presentation of papers prepared using multimedia support and discussion.
Method and Criteria of Assessment:	Assessment: Lecture: written exam at the end of semester Proseminar: passing 2 writing colloquiums, attendance in class Laboratory: passing 2 writing colloquiums and the workmanship of 9 laboratory tasks The final grade is a weighted average of the ratings of the test (50%), laboratory (25%), seminar (25%).
Course Content:	1.Calibration techniques: analytical calibration curve, method of standard additions. 2. Accuracy and precision, selectivity and sensitivity. 3. Separation techniques: general principles (retention, column efficiency, number of theoretical plates, van Deemetrs equation), classification of chromatographic methods. Gas chromatography (GC): columns and stationary phases, detectors, sample introduction system, qualitative and quantitative analysis. Temperature program, pyrolysis gas chromatography, applications. High performance liquid chromatography (HPLC): columns and stationary phases, solvents and choice of solvent systems in ion, partition, gel and adsorption chromatography, pumps, sample introduction systems, detectors, isocratic and gradient elution, qualitative and quantitative analysis. Ion chromatography: ion exchange, mobile phases, supresors, detectors. Supercritical fluid chromatography: principles and instrumentation. Electrophoresis: principles and instrumentation (capillary, buffer, detection) for CE 4. Spectrometry (spectrophotometry, AAS, AES): interaction of electromagnetic radiation with matter, electronic spectra and molecular structure, the basic notions and absorption laws, the choice of the wavelength, spectrometric methods of quantitative analysis. Analytical application of spectrophotometry. Speciation analysis. Atomic spectroscopy: principles (sources of atomic spectra) and instrumentation for spectrometric methods Atomic absorption spectroscopy: sample atomization and atomizers (flame atomization, electrothetmal atomization), atomization stages, radiation sources (hollow cathode lamps, electrodeless discharge lamps), interferences. Atomic emission spectroscopy: flame emission spectrometry, emission spectroscopy based upon plasma (inductively coupled plasma ICP), arc and spark atomization. 5. Analytical application of conductometry. Direct conductometry and conductometric titration. Analytical application of potentiometric measurements. Direct potentiometry, pehametry, potentiometric titration. 6. Electrogravimetry and coulometry: Faraday’s laws, potentiostatic and amperostatic coulometry, application of coulometric titration. 7. Polarograpic and voltammetric methods: classification of polarographic and voltammetric techniques, electrodes (HMDE, DME, SMDE, solid electrodes), polarograms, voltammograms, voltammetric currents, the basic notions (DME, polarizable electrode, over-voltage, half-wave (peak) potential, depolarizier, Ilkovic equation), currents in polarography, the supporting electrolyte, alternating current polarography, normal-pulse polarography, differential pulse polarography, square-wave polarography, principles and application of normal pulse, differential pulse, quare-wave and cyclic voltammetry, principles and application of stripping methods (anodic and cathodic stripping techniques, adsorptive stripping techniques).
Bibliography:	D. A. Skoog „Principles of Instrumental Analysis” H. H. Willard, L. L. Merritt, J. A. Dean, F. A. Settle “Instrumental Methods of Analysis” Gary D. Christian „Analytical Chemistry”, John Wiley & Sons, INC.

Classes in period "Winter Semester 2018/2019" (past)

Time span:	2018-10-01 - 2019-02-10	Selected timetable range: weekly course term Navigate to timetable
Type of class:	Discussion class, 28 hours more information Examination more information Laboratory, 56 hours more information Lecture, 14 hours more information
Coordinators:	Sławomir Domagała
Group instructors:	Sławomir Domagała
Students list:	(inaccessible to you)
Examination:	Course - (in Polish) Ocena zgodna z regulaminem studiów Discussion class - (in Polish) Ocena zgodna z regulaminem studiów Examination - (in Polish) Ocena zgodna z regulaminem studiów Laboratory - (in Polish) Ocena zgodna z regulaminem studiów Lecture - (in Polish) Zaliczenie lub ocena
(in Polish) Czy IRK BWZ?:	(in Polish) T
Teaching Method:	Lecture: a method of verbal-enriched multimedia presentation. Laboratory: practical method, the execution of the planned exercises, conversation. Seminar: word method, talk, presentation of papers prepared using multimedia support and discussion.
Method and Criteria of Assessment:	Assessment: Lecture: written exam at the end of semester Proseminar: passing 2 writing colloquiums, attendance in class Laboratory: passing 2 writing colloquiums and the workmanship of 9 laboratory tasks The final grade is a weighted average of the ratings of the test (50%), laboratory (25%), seminar (25%).
Course Content:	1.Calibration techniques: analytical calibration curve, method of standard additions. 2. Accuracy and precision, selectivity and sensitivity. 3. Separation techniques: general principles (retention, column efficiency, number of theoretical plates, van Deemetrs equation), classification of chromatographic methods. Gas chromatography (GC): columns and stationary phases, detectors, sample introduction system, qualitative and quantitative analysis. Temperature program, pyrolysis gas chromatography, applications. High performance liquid chromatography (HPLC): columns and stationary phases, solvents and choice of solvent systems in ion, partition, gel and adsorption chromatography, pumps, sample introduction systems, detectors, isocratic and gradient elution, qualitative and quantitative analysis. Ion chromatography: ion exchange, mobile phases, supresors, detectors. Supercritical fluid chromatography: principles and instrumentation. Electrophoresis: principles and instrumentation (capillary, buffer, detection) for CE 4. Spectrometry (spectrophotometry, AAS, AES): interaction of electromagnetic radiation with matter, electronic spectra and molecular structure, the basic notions and absorption laws, the choice of the wavelength, spectrometric methods of quantitative analysis. Analytical application of spectrophotometry. Speciation analysis. Atomic spectroscopy: principles (sources of atomic spectra) and instrumentation for spectrometric methods Atomic absorption spectroscopy: sample atomization and atomizers (flame atomization, electrothetmal atomization), atomization stages, radiation sources (hollow cathode lamps, electrodeless discharge lamps), interferences. Atomic emission spectroscopy: flame emission spectrometry, emission spectroscopy based upon plasma (inductively coupled plasma ICP), arc and spark atomization. 5. Analytical application of conductometry. Direct conductometry and conductometric titration. Analytical application of potentiometric measurements. Direct potentiometry, pehametry, potentiometric titration. 6. Electrogravimetry and coulometry: Faraday’s laws, potentiostatic and amperostatic coulometry, application of coulometric titration. 7. Polarograpic and voltammetric methods: classification of polarographic and voltammetric techniques, electrodes (HMDE, DME, SMDE, solid electrodes), polarograms, voltammograms, voltammetric currents, the basic notions (DME, polarizable electrode, over-voltage, half-wave (peak) potential, depolarizier, Ilkovic equation), currents in polarography, the supporting electrolyte, alternating current polarography, normal-pulse polarography, differential pulse polarography, square-wave polarography, principles and application of normal pulse, differential pulse, quare-wave and cyclic voltammetry, principles and application of stripping methods (anodic and cathodic stripping techniques, adsorptive stripping techniques).
Bibliography:	D. A. Skoog „Principles of Instrumental Analysis” H. H. Willard, L. L. Merritt, J. A. Dean, F. A. Settle “Instrumental Methods of Analysis” Gary D. Christian „Analytical Chemistry”, John Wiley & Sons, INC.

Classes in period "Winter Semester 2017/2018" (past)

Time span:	2017-10-01 - 2018-02-09	Selected timetable range: weekly course term Navigate to timetable
Type of class:	Discussion class, 28 hours more information Examination more information Laboratory, 56 hours more information Lecture, 14 hours more information
Coordinators:	Sławomir Domagała
Group instructors:	Sławomir Domagała
Students list:	(inaccessible to you)
Examination:	Course - (in Polish) Ocena zgodna z regulaminem studiów Discussion class - (in Polish) Ocena zgodna z regulaminem studiów Examination - (in Polish) Ocena zgodna z regulaminem studiów Laboratory - (in Polish) Ocena zgodna z regulaminem studiów Lecture - (in Polish) Zaliczenie lub ocena
(in Polish) Czy IRK BWZ?:	(in Polish) T
Teaching Method:	Wykład: metoda słowna-podająca wzbogacona prezentacją multimedialną. Laboratorium: metoda praktyczno-naprowadzająca, wykonanie zaplanowanych ćwiczeń, konwersacja. Konwersatorium: metoda słowno-naprowadzająca, pogadanka, prezentacja przygotowanych referatów z wykorzystaniem pomocy multimedialnych, dyskusja.
Method and Criteria of Assessment:	Assessment: Lecture: written exam at the end of semester Proseminar: passing 2 writing colloquiums, attendance in class Laboratory: passing 2 writing colloquiums and the workmanship of 9 laboratory tasks The final grade is a weighted average of the ratings of the test (50%), laboratory (25%), seminar (25%).
Course Content:	1.Calibration techniques: analytical calibration curve, method of standard additions. 2. Accuracy and precision, selectivity and sensitivity. 3. Separation techniques: general principles (retention, column efficiency, number of theoretical plates, van Deemetrs equation), classification of chromatographic methods. Gas chromatography (GC): columns and stationary phases, detectors, sample introduction system, qualitative and quantitative analysis. Temperature program, pyrolysis gas chromatography, applications. High performance liquid chromatography (HPLC): columns and stationary phases, solvents and choice of solvent systems in ion, partition, gel and adsorption chromatography, pumps, sample introduction systems, detectors, isocratic and gradient elution, qualitative and quantitative analysis. Ion chromatography: ion exchange, mobile phases, supresors, detectors. Supercritical fluid chromatography: principles and instrumentation. Electrophoresis: principles and instrumentation (capillary, buffer, detection) for CE 4. Spectrometry (spectrophotometry, AAS, AES): interaction of electromagnetic radiation with matter, electronic spectra and molecular structure, the basic notions and absorption laws, the choice of the wavelength, spectrometric methods of quantitative analysis. Analytical application of spectrophotometry. Speciation analysis. Atomic spectroscopy: principles (sources of atomic spectra) and instrumentation for spectrometric methods Atomic absorption spectroscopy: sample atomization and atomizers (flame atomization, electrothetmal atomization), atomization stages, radiation sources (hollow cathode lamps, electrodeless discharge lamps), interferences. Atomic emission spectroscopy: flame emission spectrometry, emission spectroscopy based upon plasma (inductively coupled plasma ICP), arc and spark atomization. 5. Analytical application of conductometry. Direct conductometry and conductometric titration. Analytical application of potentiometric measurements. Direct potentiometry, pehametry, potentiometric titration. 6. Electrogravimetry and coulometry: Faraday’s laws, potentiostatic and amperostatic coulometry, application of coulometric titration. 7. Polarograpic and voltammetric methods: classification of polarographic and voltammetric techniques, electrodes (HMDE, DME, SMDE, solid electrodes), polarograms, voltammograms, voltammetric currents, the basic notions (DME, polarizable electrode, over-voltage, half-wave (peak) potential, depolarizier, Ilkovic equation), currents in polarography, the supporting electrolyte, alternating current polarography, normal-pulse polarography, differential pulse polarography, square-wave polarography, principles and application of normal pulse, differential pulse, quare-wave and cyclic voltammetry, principles and application of stripping methods (anodic and cathodic stripping techniques, adsorptive stripping techniques).
Bibliography:	D. A. Skoog „Principles of Instrumental Analysis” H. H. Willard, L. L. Merritt, J. A. Dean, F. A. Settle “Instrumental Methods of Analysis” Gary D. Christian „Analytical Chemistry”, John Wiley & Sons, INC.

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Copyright by UNIVERSITY OF LODZ.