Spectroscopy

(in Polish) T

Lecture

Instructional methods: informative lecture with elements of multimedia, problematic lecture.

Seminar

Exploratory methods: classical problem method, exercise, discussion.

Laboratory

Exploratory methods: classical problem method, discussion, exercise and practical methods (experiment, experience, observation, measurement),

Expository method: demonstration.

Lecture - assessment on the basis of attendance

Seminar - graded credit: written test, activity during the course

Laboratory - graded credit: completion of exercises, completion of reports and test.

Examination - a prerequisite for taking the examination is passing the seminar and laboratory.

The final exam is carried out as a written examination (2 hours). The student receives for interpretation a set of IR, 1H-NMR, MS spectra of organic compounds and a set of questions from the compulsory material.

The condition to pass the exam is obtaining 50% of all possible points.

The overall assessment of the course includes the assessment of the components:

- exam - 40%

- Lab - 30%

- Seminar - 30%

The learning outcomes relating to knowledge (16C-2A_W03 and 16C-2A_W04) will be tested mainly in the examination.

Effects concerning skills: (16C-2A_U01) will be verified by performing exercises, reports and passing a colloquium in laboratory; (16C-2A_U04) will be verified by an exam and in seminary (final colloquium, determining the structure of 2 compounds on the basis of a set of IR, NMR and MS spectra).

The effect concerning the skills (16C-2A_U04) and social competence (16C-2A_K01, 16C-2A_K06) will be checked during the laboratory and seminary, through the assessment of the students behavior in the laboratory and evaluation of the reports from exercised - the pass mark of all the reports and the pass mark of the colloquium will be the condition to pass the laboratory. The effect 16C-2A _K04 concerning the social competence will be verified at the laboratory and seminary through the assessment of behavior and attitude towards other participants of the classes.

Lecture (14 hours):

1. Introduction to quantum chemistry and spectroscopic methods of chemical analysis. The impact of energy and matter. Energy levels of molecules. The phenomenon of energy absorption in quantitative terms.

2. Electronic spectroscopy. Absorption and emission spectra. Particle electron levels and types of electronic transitions. Chromophores in UV / VIS. Electronic spectrum prediction based on additivity rules. Construction of spectrometers and recording of spectra. The use of spectroscopy UV / VIS.

3. Infrared spectroscopy. Introduction to vibrational spectroscopy. . Harmonic and anharmonic oscillator, energy levels and wave function of two-atomic oscilator. probability of energy absorption. Types of transitions between energy levels of oscillators. Registration and interpretation of IR spectra. The use of IR spectroscopy.

4. Mass spectrometry. Physical basis of measurement of mass spectra. The ionization methods, analyzers used in mass spectrometers. Determination of the molecular weight, fragmentation processes. The use of mass spectrometry.

5. Nuclear magnetic resonance spectroscopy. The phenomenon of nuclear magnetic resonance. The physical basis for measuring the NMR spectra. Apparatus and methods for recording NMR spectra.

6. Proton magnetic resonance spectroscopy. Chemical shift. Factors influencing the chemical shift value. Spin-spin splitting, coupling constant, the signal multiplicities. Proton joins with other important nuclei. Methods to facilitate the interpretation of the NMR spectrum

Seminar (28 hours):

The aim of the seminar is to consolidate the lecture content transmitted and mainly: Learn how to interpret the spectra and their use in structural analysis of chemical compounds. During the course, students describe the spectrum of IR, 1H NMR and MS, and on this basis propose structural components of the test compounds. Based on a set of these spectra (the so-called collective tasks) offer the full structure of the test substance. Students under the direction of lead using the prepared sets of spectra of known and unknown compounds.

Laboratory (15 hours):

Registration and interpretation of spectra: Absorption and emission spectroscopy or 13 C NMR, IR, 1H-NMR and MS spectra for selected compounds

1. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spectrometric identification of organic compoundsWiley 2014.

2. W.Zieliński, A. Rajca, Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, Warszawa, 2000; i wydanie z 1995 roku.

3. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spektroskopowe metody identyfikacji związków organicznych, PWN, 2007.

(in Polish) T

Lecture

Instructional methods: informative lecture with elements of multimedia, problematic lecture.

Seminar

Exploratory methods: classical problem method, exercise, discussion.

Laboratory

Exploratory methods: classical problem method, discussion, exercise and practical methods (experiment, experience, observation, measurement),

Expository method: demonstration.

Lecture - assessment on the basis of attendance

Seminar - graded credit: written test, activity during the course

Laboratory - graded credit: completion of exercises, completion of reports and test.

Examination - a prerequisite for taking the examination is passing the seminar and laboratory.

The final exam is carried out as a written examination (2 hours). The student receives for interpretation a set of IR, 1H-NMR, MS spectra of organic compounds and a set of questions from the compulsory material.

The condition to pass the exam is obtaining 50% of all possible points.

The overall assessment of the course includes the assessment of the components:

- exam - 40%

- Lab - 30%

- Seminar - 30%

The learning outcomes relating to knowledge (16C-2A_W03 and 16C-2A_W04) will be tested mainly in the examination.

Effects concerning skills: (16C-2A_U01) will be verified by performing exercises, reports and passing a colloquium in laboratory; (16C-2A_U04) will be verified by an exam and in seminary (final colloquium, determining the structure of 2 compounds on the basis of a set of IR, NMR and MS spectra).

The effect concerning the skills (16C-2A_U04) and social competence (16C-2A_K01, 16C-2A_K06) will be checked during the laboratory and seminary, through the assessment of the students behavior in the laboratory and evaluation of the reports from exercised - the pass mark of all the reports and the pass mark of the colloquium will be the condition to pass the laboratory. The effect 16C-2A _K04 concerning the social competence will be verified at the laboratory and seminary through the assessment of behavior and attitude towards other participants of the classes.

Lecture (14 hours):

1. Introduction to quantum chemistry and spectroscopic methods of chemical analysis. The impact of energy and matter. Energy levels of molecules. The phenomenon of energy absorption in quantitative terms.

2. Electronic spectroscopy. Absorption and emission spectra. Particle electron levels and types of electronic transitions. Chromophores in UV / VIS. Electronic spectrum prediction based on additivity rules. Construction of spectrometers and recording of spectra. The use of spectroscopy UV / VIS.

3. Infrared spectroscopy. Introduction to vibrational spectroscopy. . Harmonic and anharmonic oscillator, energy levels and wave function of two-atomic oscilator. probability of energy absorption. Types of transitions between energy levels of oscillators. Registration and interpretation of IR spectra. The use of IR spectroscopy.

4. Mass spectrometry. Physical basis of measurement of mass spectra. The ionization methods, analyzers used in mass spectrometers. Determination of the molecular weight, fragmentation processes. The use of mass spectrometry.

5. Nuclear magnetic resonance spectroscopy. The phenomenon of nuclear magnetic resonance. The physical basis for measuring the NMR spectra. Apparatus and methods for recording NMR spectra.

6. Proton magnetic resonance spectroscopy. Chemical shift. Factors influencing the chemical shift value. Spin-spin splitting, coupling constant, the signal multiplicities. Proton joins with other important nuclei. Methods to facilitate the interpretation of the NMR spectrum

Seminar (28 hours):

The aim of the seminar is to consolidate the lecture content transmitted and mainly: Learn how to interpret the spectra and their use in structural analysis of chemical compounds. During the course, students describe the spectrum of IR, 1H NMR and MS, and on this basis propose structural components of the test compounds. Based on a set of these spectra (the so-called collective tasks) offer the full structure of the test substance. Students under the direction of lead using the prepared sets of spectra of known and unknown compounds.

Laboratory (15 hours):

Registration and interpretation of spectra: Absorption and emission spectroscopy or 13 C NMR, IR, 1H-NMR and MS spectra for selected compounds

1. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spectrometric identification of organic compoundsWiley 2014.

2. W.Zieliński, A. Rajca, Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, Warszawa, 2000; i wydanie z 1995 roku.

3. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spektroskopowe metody identyfikacji związków organicznych, PWN, 2007.

(in Polish) T

Lecture

Instructional methods: informative lecture with elements of multimedia, problematic lecture.

Seminar

Exploratory methods: classical problem method, exercise, discussion.

Laboratory

Exploratory methods: classical problem method, discussion, exercise and practical methods (experiment, experience, observation, measurement),

Expository method: demonstration.

Lecture - assessment on the basis of attendance

Seminar - graded credit: written test, activity during the course

Laboratory - graded credit: completion of exercises, completion of reports and test.

Examination - a prerequisite for taking the examination is passing the seminar and laboratory.

The final exam is carried out as a written examination (2 hours). The student receives for interpretation a set of IR, 1H-NMR, MS spectra of organic compounds and a set of questions from the compulsory material.

The condition to pass the exam is obtaining 50% of all possible points.

The overall assessment of the course includes the assessment of the components:

- exam - 40%

- Lab - 30%

- Seminar - 30%

The learning outcomes relating to knowledge (16C-2A_W03 and 16C-2A_W04) will be tested mainly in the examination.

Effects concerning skills: (16C-2A_U01) will be verified by performing exercises, reports and passing a colloquium in laboratory; (16C-2A_U04) will be verified by an exam and in seminary (final colloquium, determining the structure of 2 compounds on the basis of a set of IR, NMR and MS spectra).

The effect concerning the skills (16C-2A_U04) and social competence (16C-2A_K01, 16C-2A_K06) will be checked during the laboratory and seminary, through the assessment of the students behavior in the laboratory and evaluation of the reports from exercised - the pass mark of all the reports and the pass mark of the colloquium will be the condition to pass the laboratory. The effect 16C-2A _K04 concerning the social competence will be verified at the laboratory and seminary through the assessment of behavior and attitude towards other participants of the classes.

Lecture (14 hours):

1. Introduction to quantum chemistry and spectroscopic methods of chemical analysis. The impact of energy and matter. Energy levels of molecules. The phenomenon of energy absorption in quantitative terms.

2. Electronic spectroscopy. Absorption and emission spectra. Particle electron levels and types of electronic transitions. Chromophores in UV / VIS. Electronic spectrum prediction based on additivity rules. Construction of spectrometers and recording of spectra. The use of spectroscopy UV / VIS.

3. Infrared spectroscopy. Introduction to vibrational spectroscopy. . Harmonic and anharmonic oscillator, energy levels and wave function of two-atomic oscilator. probability of energy absorption. Types of transitions between energy levels of oscillators. Registration and interpretation of IR spectra. The use of IR spectroscopy.

4. Mass spectrometry. Physical basis of measurement of mass spectra. The ionization methods, analyzers used in mass spectrometers. Determination of the molecular weight, fragmentation processes. The use of mass spectrometry.

5. Nuclear magnetic resonance spectroscopy. The phenomenon of nuclear magnetic resonance. The physical basis for measuring the NMR spectra. Apparatus and methods for recording NMR spectra.

6. Proton magnetic resonance spectroscopy. Chemical shift. Factors influencing the chemical shift value. Spin-spin splitting, coupling constant, the signal multiplicities. Proton joins with other important nuclei. Methods to facilitate the interpretation of the NMR spectrum

Seminar (28 hours):

The aim of the seminar is to consolidate the lecture content transmitted and mainly: Learn how to interpret the spectra and their use in structural analysis of chemical compounds. During the course, students describe the spectrum of IR, 1H NMR and MS, and on this basis propose structural components of the test compounds. Based on a set of these spectra (the so-called collective tasks) offer the full structure of the test substance. Students under the direction of lead using the prepared sets of spectra of known and unknown compounds.

Laboratory (15 hours):

Registration and interpretation of spectra: Absorption and emission spectroscopy or 13 C NMR, IR, 1H-NMR and MS spectra for selected compounds

1. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spectrometric identification of organic compoundsWiley 2014.

2. W.Zieliński, A. Rajca, Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, Warszawa, 2000; i wydanie z 1995 roku.

3. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spektroskopowe metody identyfikacji związków organicznych, PWN, 2007.

(in Polish) T

(in Polish) T

Lecture: a method of verbal-enriched multimedia presentation.

Laboratory: practical method, the execution of the planned exercises, conversation.

Seminar: word method, talk.

Lecture - based on the presence and activity during the course

Seminar - written test, and on the basis of activity during the course

Laboratory - on the basis of activity during the course

Final examination carried out as a written exam (1 hour). Student is given a set of spectra (IR and 1H-NMR) of particular organic compound to determine the chemical structure and a set of questions of material transferred during lecture .

The overall assessment of the course includes the assessment of the components:

- exam - 40%

- Lab - 30%

- Seminar - 30%

Lecture:

1. Introduction to quantum chemistry and spectroscopic methods of chemical analysis. The impact of energy and matter. Energy levels of molecules. The phenomenon of energy absorption in quantitative terms.

2. Electronic spectroscopy. Absorption and emission spectra. Particle electron levels and types of electronic transitions. Chromophores in UV / VIS. Electronic spectrum prediction based on additivity rules. Construction of spectrometers and recording of spectra. The use of spectroscopy UV / VIS.

3. Infrared spectroscopy. Introduction to vibrational spectroscopy. . Harmonic and anharmonic oscillator, energy levels and wave function of two-atomic oscilator. probability of energy absorption. Types of transitions between energy levels of oscillators. Registration and interpretation of IR spectra. The use of IR spectroscopy.

4. Mass spectrometry. Physical basis of measurement of mass spectra. The ionization methods, analyzers used in mass spectrometers. Determination of the molecular weight, fragmentation processes. The use of mass spectrometry.

5. Nuclear magnetic resonance spectroscopy. The phenomenon of nuclear magnetic resonance. The physical basis for measuring the NMR spectra. Apparatus and methods for recording NMR spectra.

6. Proton magnetic resonance spectroscopy. Chemical shift. Factors influencing the chemical shift value. Spin-spin splitting, coupling constant, the signal multiplicities. Proton joins with other important nuclei. Methods to facilitate the interpretation of the NMR spectrum

Seminar:

The aim of the seminar is to consolidate the lecture content transmitted and mainly: Learn how to interpret the spectra and their use in structural analysis of chemical compounds. During the course, students describe the spectrum of IR, NMR and MS, and on this basis propose structural components of the test compounds. Based on a set of these spectra (the so-called collective tasks) offer the full structure of the test substance. Students under the direction of lead using the prepared sets of spectra of known and unknown compounds.

Laboratory:

Registration and interpretation of Absorption and emission spectroscopy, IR, 1H-NMR and MS spectra for selected compounds.

1. W.Zieliński, A. Rajca, Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, Warszawa, 2000; i wydanie z 1995 roku.

2. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spektroskopowe metody identyfikacji związków organicznych, PWN, 2007

(in Polish) T

Lecture: a method of verbal-enriched multimedia presentation.

Laboratory: practical method, the execution of the planned exercises, conversation.

Seminar: word method, talk.

Lecture - based on the presence and activity during the course

Seminar - written test, and on the basis of activity during the course

Laboratory - on the basis of activity during the course

Final examination carried out as a written exam (1 hour). Student is given a set of spectra (IR and 1H-NMR) of particular organic compound to determine the chemical structure and a set of questions of material transferred during lecture .

The overall assessment of the course includes the assessment of the components:

- exam - 40%

- Lab - 30%

- Seminar - 30%

Lecture:

1. Introduction to quantum chemistry and spectroscopic methods of chemical analysis. The impact of energy and matter. Energy levels of molecules. The phenomenon of energy absorption in quantitative terms.

2. Electronic spectroscopy. Absorption and emission spectra. Particle electron levels and types of electronic transitions. Chromophores in UV / VIS. Electronic spectrum prediction based on additivity rules. Construction of spectrometers and recording of spectra. The use of spectroscopy UV / VIS.

3. Infrared spectroscopy. Introduction to vibrational spectroscopy. . Harmonic and anharmonic oscillator, energy levels and wave function of two-atomic oscilator. probability of energy absorption. Types of transitions between energy levels of oscillators. Registration and interpretation of IR spectra. The use of IR spectroscopy.

4. Mass spectrometry. Physical basis of measurement of mass spectra. The ionization methods, analyzers used in mass spectrometers. Determination of the molecular weight, fragmentation processes. The use of mass spectrometry.

5. Nuclear magnetic resonance spectroscopy. The phenomenon of nuclear magnetic resonance. The physical basis for measuring the NMR spectra. Apparatus and methods for recording NMR spectra.

6. Proton magnetic resonance spectroscopy. Chemical shift. Factors influencing the chemical shift value. Spin-spin splitting, coupling constant, the signal multiplicities. Proton joins with other important nuclei. Methods to facilitate the interpretation of the NMR spectrum

Seminar:

The aim of the seminar is to consolidate the lecture content transmitted and mainly: Learn how to interpret the spectra and their use in structural analysis of chemical compounds. During the course, students describe the spectrum of IR, NMR and MS, and on this basis propose structural components of the test compounds. Based on a set of these spectra (the so-called collective tasks) offer the full structure of the test substance. Students under the direction of lead using the prepared sets of spectra of known and unknown compounds.

Laboratory:

Registration and interpretation of Absorption and emission spectroscopy, IR, 1H-NMR and MS spectra for selected compounds.

1. W.Zieliński, A. Rajca, Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, Warszawa, 2000; i wydanie z 1995 roku.

2. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spektroskopowe metody identyfikacji związków organicznych, PWN, 2007

(in Polish) T

Lecture: a method of verbal-enriched multimedia presentation.

Laboratory: practical method, the execution of the planned exercises, conversation.

Seminar: word method, talk.

Lecture - based on the presence and activity during the course

Seminar - written test, and on the basis of activity during the course

Laboratory - on the basis of activity during the course

Final examination carried out as a written exam (1 hour). Student is given a set of spectra (IR and 1H-NMR) of particular organic compound to determine the chemical structure and a set of questions of material transferred during lecture .

The overall assessment of the course includes the assessment of the components:

- exam - 40%

- Lab - 30%

- Seminar - 30%

Lecture:

1. Introduction to quantum chemistry and spectroscopic methods of chemical analysis. The impact of energy and matter. Energy levels of molecules. The phenomenon of energy absorption in quantitative terms.

2. Electronic spectroscopy. Absorption and emission spectra. Particle electron levels and types of electronic transitions. Chromophores in UV / VIS. Electronic spectrum prediction based on additivity rules. Construction of spectrometers and recording of spectra. The use of spectroscopy UV / VIS.

3. Infrared spectroscopy. Introduction to vibrational spectroscopy. . Harmonic and anharmonic oscillator, energy levels and wave function of two-atomic oscilator. probability of energy absorption. Types of transitions between energy levels of oscillators. Registration and interpretation of IR spectra. The use of IR spectroscopy.

4. Mass spectrometry. Physical basis of measurement of mass spectra. The ionization methods, analyzers used in mass spectrometers. Determination of the molecular weight, fragmentation processes. The use of mass spectrometry.

5. Nuclear magnetic resonance spectroscopy. The phenomenon of nuclear magnetic resonance. The physical basis for measuring the NMR spectra. Apparatus and methods for recording NMR spectra.

6. Proton magnetic resonance spectroscopy. Chemical shift. Factors influencing the chemical shift value. Spin-spin splitting, coupling constant, the signal multiplicities. Proton joins with other important nuclei. Methods to facilitate the interpretation of the NMR spectrum

Seminar:

The aim of the seminar is to consolidate the lecture content transmitted and mainly: Learn how to interpret the spectra and their use in structural analysis of chemical compounds. During the course, students describe the spectrum of IR, NMR and MS, and on this basis propose structural components of the test compounds. Based on a set of these spectra (the so-called collective tasks) offer the full structure of the test substance. Students under the direction of lead using the prepared sets of spectra of known and unknown compounds.

Laboratory:

Registration and interpretation of Absorption and emission spectroscopy, IR, 1H-NMR and MS spectra for selected compounds.

1. W.Zieliński, A. Rajca, Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, Warszawa, 2000; i wydanie z 1995 roku.

2. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spektroskopowe metody identyfikacji związków organicznych, PWN, 2007

(in Polish) T

Lecture: a method of verbal-enriched multimedia presentation.

Laboratory: practical method, the execution of the planned exercises, conversation.

Seminar: word method, talk.

Lecture - based on the presence and activity during the course

Seminar - written test, and on the basis of activity during the course

Laboratory - written test ( pass the assessment in accordance with the Rules of Study )

Final examination carried out as a written exam (3 hours). Student is given a set of spectra (IR and 1H-NMR) of particular organic compound to determine the chemical structure and a set of questions of material transferred during lecture .

The overall assessment of the course includes the assessment of the components:

- exam - 40%

- Lab - 30%

- Seminar - 30%

Lecture:

1. Introduction to quantum chemistry and spectroscopic methods of chemical analysis. The impact of energy and matter. Energy levels of molecules. The phenomenon of energy absorption in quantitative terms.

2. Electronic spectroscopy. Absorption and emission spectra. Particle electron levels and types of electronic transitions. Chromophores in UV / VIS. Electronic spectrum prediction based on additivity rules. Construction of spectrometers and recording of spectra. The use of spectroscopy UV / VIS.

3. Infrared spectroscopy. Introduction to vibrational spectroscopy. . Harmonic and anharmonic oscillator, energy levels and wave function of two-atomic oscilator. probability of energy absorption. Types of transitions between energy levels of oscillators. Registration and interpretation of IR spectra. The use of IR spectroscopy.

4. Mass spectrometry. Physical basis of measurement of mass spectra. The ionization methods, analyzers used in mass spectrometers. Determination of the molecular weight, fragmentation processes. The use of mass spectrometry.

5. Nuclear magnetic resonance spectroscopy. The phenomenon of nuclear magnetic resonance. The physical basis for measuring the NMR spectra. Apparatus and methods for recording NMR spectra.

6. Proton magnetic resonance spectroscopy. Chemical shift. Factors influencing the chemical shift value. Spin-spin splitting, coupling constant, the signal multiplicities. Proton joins with other important nuclei. Methods to facilitate the interpretation of the NMR spectrum

Seminar:

The aim of the seminar is to consolidate the lecture content transmitted and mainly: Learn how to interpret the spectra and their use in structural analysis of chemical compounds. During the course, students describe the spectrum of IR, NMR and MS, and on this basis propose structural components of the test compounds. Based on a set of these spectra (the so-called collective tasks) offer the full structure of the test substance. Students under the direction of lead using the prepared sets of spectra of known and unknown compounds.

Laboratory:

Registration and interpretation of Absorption and emission spectroscopy, IR, 1H-NMR and MS spectra for selected compounds.

1. W.Zieliński, A. Rajca, Metody spektroskopowe i ich zastosowanie do identyfikacji związków organicznych, WNT, Warszawa, 2000; i wydanie z 1995 roku.

2. R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spektroskopowe metody identyfikacji związków organicznych, PWN, 2007